Table 1. The Composition of PU Samples Used in this Hydrolysis Experiment

Sample No. 1,4-BD Isocyanate wt. (g) DMSO wt. (g) DBTDL wt. (g) Solid content (wt.%)
S1 94.63 (90.12×1.05)* MDI 250.25 3090 0.60 10.0
S2 TDI 174.26 2407 0.46 10.0
S3 H12MDI 262.40 1646 0.50 17.8
S4 IPDI 222.31 1388 0.46 18.6
S5 HDI 168.28 1189 0.37 18.1
The molar ratio of diisocyanates to 1,4-BD was kept 1.05 for all PU samples.